HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Diacetylbenzene → alpha1,alpha3-Dimethyl-1,3-benzenedimethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Diacetylbenzene | HCID 23229 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Product | alpha1,alpha3-Dimethyl-1,3-benzenedimethanol | HCID 15148377 | — |
Reaction Steps
This mixture of stereoisomers was prepared from 1,3-diacetylbenzene by reduction with sodium borohydride as described above for the para stereoisomers. The mixture of stereoisomers was isolated as a semisolid. It appeared as a single spot on TLC and as a single peak on VPC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05280096 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-828293c7f29e4075b17cc23d840ed7d7 |
| Source note | uspto-grants-1994_01 |