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Potassium Carbonate → HCID 178442094、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 4'-Pentyl-2,3-difluorobiphenyl-4-ol | HCID 19103643 | — |
| 反応物 | HCID 178444521 | HCID 178444521 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | HCID 178442094 | HCID 178442094 | — |
反応手順
0.1 mol of 4'-n-pentyl-2,3-difluorobiphenyl-4-ol and 0.1 mol of trans-4-n-pentylcyclohexylmethyl iodide and heated in the presence of 0.12 mol of anhydrous K2CO3 in dimethylformamide (DMF) until the mixture boils gently. When the reaction has ended, the mixture is worked up in the customary manner and the product is purified by chromatography and crystallization. Trans-4-n-pentylcyclohexylmethyl 4'-pentyl-2,3-difluorobiphenyl-4-yl ether is obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05279764 |
| 出典データセット | uspto-grants-1994_01 |
| ORD ID | ord-45da8cae7649494cbef17b87fd5a88e3 |
| 出典メモ | uspto-grants-1994_01 |