HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl Isothiocyanate → HCID 5361886, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl Isothiocyanate | HCID 5971 | — |
| Reactant | HCID 474761 | HCID 474761 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 5361886 | HCID 5361886 | 53.3% |
Reaction Steps
A solution of 2.7 g (0.02 mol) of 2-acetylpyridine hydrazone in 5 ml of MeOH was treated with 3.1 g (0.03 mol) of allyl isothiocyanate and the solution was heated at reflux for 3 hours. The solution was cooled and the product which formed was collected. The crude material was recrystallized 3 times from MeOH, affording 2.5 g (49%) of white needles of 2-acetylpyridine 4-allyl-3-thiosemicarbazone, mp 107° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05281597 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-bcecfb6751ff4227a0ec4e71103e1378 |
| Source note | uspto-grants-1994_01 |