HuagongsheHuagongshe Chemistry Print Report · For research reference only
Octanal → HCID 11063309, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Octanal | HCID 454 | — |
| Reactant | Cyclopentanone | HCID 8452 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 11063309 | HCID 11063309 | — |
Reaction Steps
The procedure was similar to that in Example 1 by reacting n-octanal with cyclopentanone in the presence of 1% NaOH to give 2-(E)-octylidene cyclopentanone. The boiling point of this intermediate compound was determined to be 120°-125° C. at a pressure of 4 mm Hg. A subsequent Mannich reaction yielded the 2-Dimethylaminomethyl-5-(E)-octylidene cyclopentanone hydrochloride. The melting point of the product was determined to be 138°-140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05281622 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-e334e9397c014eccad1d53635a6616ce |
| Source note | uspto-grants-1994_01 |