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HRID1198704

反应详情

EQUATION

反应方程式

HRID 1198704 的结构方程式

REACTANTS

反应物

2
结构：Fc1cc(Br)ccc1CBr
HCID2733660

4-Bromo-1-(bromomethyl)-2-fluoro-benzene

C7H5Br2F

结构：CCCCc1nn(-c2cc([N+](=O)[O-])ccc2Cl)c(=O)[nH]1
HCID135464101

未命名化合物

PRODUCTS

生成物

1
结构：CCCCc1nn(-c2cc([N+](=O)[O-])ccc2Cl)c(=O)n1Cc1ccc(Br)cc1F
HCID19939472

未命名化合物

收率 79%

PROCEDURE

实验过程

By the procedure of Example 28, Step D, 5-n-butyl-2-(2-chloro-5-nitrophenyl)-2,4-dihydro-3H-1,2,4-triazol-3-one (from Example 24, Step A) was alkylated with 4-bromo-2-fluorobenzyl bromide to give a 79% yield of the title compound as an off-white foam, homogeneous by TLC in 4:1 hexane-EtOAc; mass spectrum (FAB) m/e 483, 485 (M+1)+.