HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 10842123, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 10817689 | HCID 10817689 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 10842123 | HCID 10842123 | — |
Reaction Steps
To a solution alcohol (300 mg) from Step 4 in Ac2O (2 mL) was added pyridine (300 mL) and DMAP (2 mg). After 2 hr, the reaction mixture was diluted with Et2O, washed with H2O, a solution of CuSO4, and the solvent evaporated to give the title product which was used as such for the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05281720 |
| Source dataset | uspto-grants-1994_01 |
| ORD ID | ord-08c27a7ed19748c2afe115ca5dbf9d22 |
| Source note | uspto-grants-1994_01 |