HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylsilyl cyanide → HCID 14850772, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylsilyl cyanide | HCID 82115 | — |
| Reactant | HCID 14850771 | HCID 14850771 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 14850772 | HCID 14850772 | — |
Reaction Steps
A mixture of 5.9 g of 4-(diethylphosphonomethyl)-quinoline-N-oxide, 15 ml of trimethylsilyl cyanide and 7 ml of triethylamine is heated at 80° for 1 hour and evaporated to dryness. The residue is purified by chromatography on silica gel using methanol/methylene chloride (5:95) as eluent to yield 4-(diethylphosphonomethyl)-2-cyanoquinoline as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04898854 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-6b792d9275cb49e38d5fa55cd90087a0 |
| Source note | uspto-grants-1990_02 |