HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14850765, compound → HCID 14850766, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14850765 | HCID 14850765 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 14850766 | HCID 14850766 | — |
Reaction Steps
A mixture of 348 mg of 3-phosphonopyridine-2-carboxylic acid hydrochloride and 100 mg of Adams catalyst in dilute aqueous acetic acid is hydrogenated at 3 atmospheres pressure and room temperature to yield 3-phosphonopiperidine-2-carboxylic acid, mp 150° dec.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04898854 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-d158cfcf0a0c4e41a9b5a9b6f3f43383 |
| Source note | uspto-grants-1990_02 |