Sodium Carbonate → HCID 131716310, compound

HRID 1198943Notes

Reaction equation

HRID 1198943 reaction equation
[CH3:1][CH:2]1[C:11]2[CH:10]=[C:9]([NH2:12])[CH2:8][C:7]([CH3:14])([CH3:13])[C:6]=2[NH:5][C:4](=[O:15])[CH2:3]1.F[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=1[N+:23]([O-:25])=[O:24].C(=O)([O-])[O-].[Na+].[Na+]>>[CH3:1][CH:2]1[C:11]2[CH:10]=[C:9]([NH:12][C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=3[N+:23]([O-:25])=[O:24])[CH2:8][C:7]([CH3:14])([CH3:13])[C:6]=2[NH:5][C:4](=[O:15])[CH2:3]1

Participants

4

Reactant 3

HCID 10340Sodium CarbonateHCID 738951-Fluoro-2-nitrobenzeneHCID 68112686HCID 68112686, compound

Product 1

HCID 131716310HCID 131716310, compound

Procedure

This compound, m.p. 205°14 211°, was prepared similarly to Preparation 20 using 3,4-dihydro-4,8,8-trimethyl-6-amino-2-(1H)-quinolone, 1-fluoro-2-nitrobenzene, and sodium carbonate as starting materials.

Workup

  1. custom205°14 211°

Sources & evidence

ORD record
ord-16e1f4ff81fe44c38932169ca63998b8
Source dataset
uspto-grants-1990_02
Patent number
US04898872

Reaction notes

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