Hydrochloric Acid → HCID 14835401, compound

Participants

Reaction Steps

A solution of 400 mg (0.00125 mole) of 3-(4-chlorobenzoyl)-4-nitrobenzene acetamide in 20 ml of tetrahydrofuran was warmed to 50° C. and treated with 1 g of tin powder and 1 ml of concentrated hydrochloric acid. The mixture was stirred for 1 hr, then filtered. The filtrate was poured into water and the solid was collected and recrystallized from ethanol-isopropanol to give 50 mg (14%) of light-yellow crystals, m.p. 242.0°-43.5° C.

Provenance & Evidence