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HRID1199235

反应详情

EQUATION

反应方程式

HRID 1199235 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)NCC(=O)NCC(=O)O
HCID333466

N-(tert-butoxycarbonyl)glycylglycine

C9H16N2O5

结构：CC(C)[C@H](NC(=O)CNC(=O)CNC(=O)OC(C)(C)C)C(=O)N1CCC[C@H]1C(=O)OCc1ccccc1
HCID14306249

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)[C@H](NC(=O)CNC(=O)CNC(=O)OC(C)(C)C)C(=O)N1CCC[C@H]1C(=O)O
HCID14306251

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

IV (6.2 g, 0.012 mole) in acetic acid was hydrogenated and worked up as for II to obtain V quantitatively, no sharp m.p. 743°-783° C. Rf3, 0.25; Rf4, 0.15. Anal. Calcd. for C19H32N4O7 : C, 51.10; H, 7.67; N, 12.54%. Found: C, 51.28: H, 7.50, N, 12.38%.

WORKUP

后处理

  1. customto obtain V quantitatively