Cumen hydroperoxide → 2-Propanone, reaction products with phenol

HRID 1199254Notes

Reaction equation

HRID 1199254 reaction equation
[O-:1]O.[C:3]1([CH:9](C)C)[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1>CC(C)=O>[C:3]1([OH:1])[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[CH3:4][C:3]([CH3:9])=[O:1]

Participants

3

Reactant 1

HCID 53627471Cumen hydroperoxide

Product 1

HCID 544642892-Propanone, reaction products with phenol

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Conditions

Temperature
66 °C

Procedure

Following the procedures of Comparative Example A, 40.0 g of "80%" cumene hydroperoxide is diluted with acetone (60.0 g) and heated to reflux (66° C.) in the absence of any added clay catalyst.

Workup

  1. temperatureheated

Sources & evidence

ORD record
ord-7b3a97ab985245d3b5309bc5b9286274
Source dataset
uspto-grants-1990_02
Patent number
US04898987

Reaction notes

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