Diethylamine → HCID 19813947, compound

Participants

Reaction Steps

Under a blanket of nitrogen, a mixture of 55 g (0.180 moles) of perfluorobutane sulfonyl fluoride and 70.7 g (0.970 moles) of diethylamine was heated at reflux for nine hours. The reaction mixture was dissolved in 600 ml of ether and percolated through a column of 60 g of acidic alumina. The ether was stripped and the product was distilled at 56°-58° C. at 2.0 mm. Yield 41.6 g (65%).

Provenance & Evidence