Sodium Hydroxide → HCID 23710092, compound

Participants

Reaction Steps

To a solution of 1.17 g (3.14 mmoles) of the lactone prepared in Step 11, and 21 ml of ethanol was added 3.14 ml of 1N NaOH (3.14 mmoles). After stirring for 30 minutes, the ethanol was removed in vacuo. The residue was redissolved in 50 ml of HPLC grade H2O and extracted twice with hexane. The water layer was freeze-dried to yield a white powder. M.P. 160°-190° C. (dec).

Provenance & Evidence