HuagongsheHuagongshe Chemistry Print Report · For research reference only
Homoveratrylamine → HCID 86743753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Homoveratrylamine | HCID 8421 | — |
| Reactant | 2-Methylbenzenecarbothioyl chloride | HCID 12849389 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86743753 | HCID 86743753 | — |
Reaction Steps
2-(3,4-Dimethoxyphenyl)ethylamine (4.8 ml), poly(4-vinylpyridine) (PVP) (5.7 g) and 2-methylthiobenzoyl chloride (5.3 g) were stirred in dichloromethane (50 ml) with cooling in a water bath at 20° for one night. The PVP was filtered off and washed with CHCl3. Evaporation of the extracts followed by flash chromatography (ethyl acetate/petroleum ether) gave the sub-title compound, mp 94°-95°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04900751 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-65fe77d0203747908fbc31567c7a28f4 |
| Source note | uspto-grants-1990_02 |