2,6-Dichlorobenzyl chloride → HCID 54248276, compound

HRID 1199477Notes

Reaction equation

HRID 1199477 reaction equation
[CH2:1]([NH:4][C:5]1[N:13]=[CH:12][N:11]=[C:10]2[C:6]=1[NH:7][CH:8]=[N:9]2)[CH2:2][CH3:3].[Cl:14][C:15]1[CH:22]=[CH:21][CH:20]=[C:19]([Cl:23])[C:16]=1[CH2:17]Cl>>[Cl:14][C:15]1[CH:22]=[CH:21][CH:20]=[C:19]([Cl:23])[C:16]=1[CH2:17][N:9]1[CH:8]=[N:7][C:6]2[C:10]1=[N:11][CH:12]=[N:13][C:5]=2[NH:4][CH2:1][CH2:2][CH3:3]

Participants

3

Reactant 2

HCID 748322,6-Dichlorobenzyl chlorideHCID 2155040HCID 2155040, compound

Product 1

HCID 54248276HCID 54248276, compound

Procedure

Exploying N6 -n-propyladenine prepared in Example 16 and 2,6-dichlorobenzyl chloride, the same procedures as in Example 39, (1) were repeated to give a crude 9-(2,6-dichlorobenzyl)-N6 -n-propyladenine, in which the purity was 72.6% by weight and the content of the 3-isomer was 27.4% by weight.

Sources & evidence

ORD record
ord-ab1734a3c3bb491ebcb508d989f7b6da
Source dataset
uspto-grants-1990_02
Patent number
US04900826

Reaction notes

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