HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 8-methyl-6-(1,2,4-triazol-4-yl)-2-(1H)-quinolone hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-Methoxy-8-methyl-6-(1,2,4-triazol-4-yl)-quinoline | HCID 19867067 | — |
| Product | 8-methyl-6-(1,2,4-triazol-4-yl)-2-(1H)-quinolone hydrochloride | HCID 131715460 | — |
Reaction Steps
The following compound, m.p. >350°, was prepared similarly to the previous Example, starting from 2-methoxy-8-methyl-6-(1,2,4-triazol-4-yl)-quinoline and 5M HCl, except that, after refluxing the methoxy starting material with 5M HCl and cooling, the hydrochloride 1/2 hydrate crystallised out of solution and was filtered off and dried. ##STR60##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04900839 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-91d224b4e6444b4f91bafecddb7da85f |
| Source note | uspto-grants-1990_02 |