Silver Nitrate → HCID 178418580, compound

HRID 1199634Notes

Reaction equation

HRID 1199634 reaction equation
[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[N:2]1.[N+]([O-])([O-])=O.[Ag+:14]>O>[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[N:2]1.[Ag:14]

Participants

4

Reactant 2

HCID 24470Silver NitrateHCID 178418385HCID 178418385, compound

Product 1

HCID 178418580HCID 178418580, compoundYield 1,760.9%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

In 3,000 ml of water were dissolved 28 g of gelatin and 13.2 g of benzotriazole, and the solution was kept at 40° C. under stirring. A solution of 17 g of silver nitrate in 100 ml of water was added to the gelatin aqueous solution over a period of 2 minutes. The excess salt was sedimented and removed by adjusting to a pH of 4.0. The emulsion was adjusted to a pH of 6.30 to obtain 400 g of a silver benzotriazole emulsion.

Workup

  1. customwas kept at 40° C.
  2. customremoved

Sources & evidence

ORD record
ord-172e4013f60e46e4968da673a7146ed8
Source dataset
uspto-grants-1990_02
Patent number
US04902599

Reaction notes

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