HuagongsheHuagongshe Chemistry Print Report · For research reference only
Calcium Carbonate → HCID 178419798, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Calcium Carbonate | HCID 10112 | — |
| Reactant | Sulfur | HCID 5362487 | — |
| Reactant | endo-Dicyclopentadiene | HCID 15618652 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178419798 | HCID 178419798 | — |
Reaction Conditions
| Temperature | 150 °C |
|---|
Reaction Steps
Into a 4 liter autoclave were placed 425 g of sulfur, 75 g of DCPD, 2500 ml of water, 20 g of calcium carbonate and 5.0 g of Igepal®-630 (GAF). The reactor was sealed and heated to 150° C. for three hours with stirring. After cooling to room temperature, the sulfur/DCPD adduct was isolated as small ribbons.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04902775 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-f337de8edcc0485a8be6120165475b16 |
| Source note | uspto-grants-1990_02 |