HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → Ditridecyl 2-bromosuccinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 1-Tridecanol | HCID 8207 | — |
| Reactant | Bromosuccinic acid | HCID 73557 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Ditridecyl 2-bromosuccinate | HCID 20072149 | — |
Reaction Steps
A mixture of 19.7 g. (0.1 mole) of bromosuccinic acid, 40.1 g. (0.2 mole) of tridecanol, 0.25 g. of p-toluenesulfonic acid and 200 ml. of toluene is refluxed for 7 hours, using a Dean-Stark trap. There is collected 3.6 ml. of H2O in the trap which is exactly the calculated amount for this reaction when completed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04902804 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-467e94572fd34f74b19f18af15a52433 |
| Source note | uspto-grants-1990_02 |