HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 97094-83-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 2-Chloro-5-nitrobenzenesulfonyl chloride | HCID 20630 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Product | 97094-83-2 | HCID 4713013 | — |
Reaction Steps
For production of the compound (III), 2-chloro-5-nitrobenzenesulfonyl chloride, i.e. the compound (V), is first reacted with stannous chloride and hydrochloric acid or with zinc and hydrochloric acid or sulfuric acid at a temperature of 40° to 100° C. to give 2-chloro-5-aminothiophenol, i.e. the compound (IV). The amount of the stannous chloride or zinc is usually from 6 to 10 equivalents to the compound (V).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04902832 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-3296a01d55434617a98a3d69479fe7fa |
| Source note | uspto-grants-1990_02 |