HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → 2-(beta-Hydroxyethoxy)-4-methylamino-5-nitrophenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | N-methyl-6-nitro-1,3-dioxaindan-5-amine | HCID 13742671 | — |
| Product | 2-(beta-Hydroxyethoxy)-4-methylamino-5-nitrophenol | HCID 13742678 | — |
Reaction Steps
0.06 mol (3.9 g) of 85% pure potassium hydroxide pellets is dissolved in 60 ml of ethylene glycol on a boiling water bath. 0.03 mol (5.9 g) of 2-methylamino-4,5-methylenedioxy-1-nitrobenzene, prepared according to Example 3, is added with stirring in the course of 5 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04904276 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-7eb4ad7672d2483a9e9560e4ad2db472 |
| Source note | uspto-grants-1990_02 |