Sodium Methoxide → HCID 70373563, compound

HRID 1199874Notes

Reaction equation

HRID 1199874 reaction equation
C([NH:5][C:6]1[CH:11]=[C:10]2[O:12][CH2:13][O:14][C:9]2=[CH:8][C:7]=1[N+:15]([O-:17])=[O:16])CCC.C[O-].[Na+]>CO>[CH3:13][O:12][CH:10]([CH2:11][CH2:6][NH2:5])[CH3:9].[N+:15]([C:7]1[CH:6]=[CH:11][CH:10]=[C:9]([OH:14])[CH:8]=1)([O-:17])=[O:16]

Participants

4

Reactant 2

HCID 10942334Sodium MethoxideHCID 137426722-n-Butylamino-4,5-methylenedioxy-1-nitrobenzene

Product 1

HCID 70373563HCID 70373563, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

A solution of 0.03 mol (6.9 g) of 2-n-butylamino-4,5-methylenedioxy-1-nitrobenzene, prepared according to Example 4, in 45 ml of a 30% strength solution of sodium methylate in methanol is brought for 15 minutes to the refluxing temperature of the methanol.

Sources & evidence

ORD record
ord-42eabb6649f94ec2a5bf9e5e6d78ab6d
Source dataset
uspto-grants-1990_02
Patent number
US04904276

Reaction notes

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