Sodium Methoxide → HCID 13742680, compound

HRID 1199875Notes

Reaction equation

HRID 1199875 reaction equation
[OH:1][CH2:2][CH2:3][CH2:4][NH:5][C:6]1[CH:11]=[C:10]2[O:12][CH2:13][O:14][C:9]2=[CH:8][C:7]=1[N+:15]([O-:17])=[O:16].C[O-].[Na+]>CO>[CH3:13][O:12][C:10]1[CH:11]=[C:6]([NH:5][CH2:4][CH2:3][CH2:2][OH:1])[C:7]([N+:15]([O-:17])=[O:16])=[CH:8][C:9]=1[OH:14]

Participants

4

Reactant 2

HCID 10942334Sodium MethoxideHCID 13742673HCID 13742673, compound

Product 1

HCID 13742680HCID 13742680, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

A mixture consisting of 0.013 mol (3.12 g) of 2-(γ-hydroxypropyl)amino-4,5-methylenedioxy-1-nitrobenzene, prepared according to Example 5, and 22 ml of a 30% strength solution of sodium methylate in methanol are brought to the refluxing temperature of the methanol for 10 minutes.

Workup

  1. customprepared

Sources & evidence

ORD record
ord-31d155747d224c6fa9902b5110b4c93d
Source dataset
uspto-grants-1990_02
Patent number
US04904276

Reaction notes

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