HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dichlorobenzoic acid → HCID 178478547, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dichlorobenzoic acid | HCID 5811 | — |
| Reactant | 3,4-Diaminopyridine | HCID 5918 | — |
| Product | HCID 178478547 | HCID 178478547 | — |
Reaction Steps
When 3,5-dichlorobenzoic acid and 3,4-diaminopyridine were reacted according to the procedure in Example 1, the title compound (base) was obtained. Upon converting to the hydrochloride salt and crystallization from ethanol/dimethylformamide/water, a 61% yield of pure 2-(3,5-dichlorophenyl)imidazo[4,5-c]pyridine hydrochloride was obtained as cream-colored needles, m.p. >320° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04904785 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-331b65c2777d4d93a283c0061e220fb9 |
| Source note | uspto-grants-1990_02 |