HuagongsheHuagongshe Chemistry Print Report · For research reference only
Alpha-Methylstyrene → HCID 19865016, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Alpha-Methylstyrene | HCID 7407 | — |
| Reactant | Perchloric Acid | HCID 24247 | — |
| Reactant | HCID 19864939 | HCID 19864939 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19865016 | HCID 19865016 | — |
Reaction Steps
5.0 Parts of 2-methyl-4-(5-methoxycarbonyl-2-methyl-pent-2-yl)-phenol, 2.4 parts of α-methylstyrene, and 0.5 parts of 70% perchloric acid in 25 parts of methylene chloride were reacted and worked up as described in Example 61. Distillation gave methyl 5-(3-cumyl-4-hydroxy-5-methyl-phenyl)5-methyl-hexanoate, b0.7 210°-4° C. as an oil with the following percentage composition by weight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04904815 |
| Source dataset | uspto-grants-1990_02 |
| ORD ID | ord-507a3c4619ce4c08813f4b77d1f0ae33 |
| Source note | uspto-grants-1990_02 |