HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylcarbodiimide → Pent-4-ynoylaminooxy-acetic Acid Ethyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | 2-Aminoxy-acetic acid ethyl ester | HCID 19808 | — |
| Reactant | 4-Pentynoic acid | HCID 22464 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Pent-4-ynoylaminooxy-acetic Acid Ethyl Ester | HCID 59336531 | — |
Reaction Steps
To a solution of 2-Aminoxy-acetic acid ethyl ester (573 mg, 4.8 mmol) and 4-Pentynoic acid (441 mg, 4.5 mmol) in 15 mL EtOAc were added dicyclohexylcarbodiimide (928 mg, 4.5 mmol) and the resulting mixture was stirred at room temperature for 16 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07727713B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-128be03e30fc479198b6496eaff8785b |
| Source note | uspto-grants-2010_06 |