HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Chloro-9H-beta-carbolin-8-amine → (S)-5-(6-Chloro-9H-beta-carbolin-8-ylcarbamoyl)-2,2-dimethyl-morpholine-4-carboxylic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Chloro-9H-beta-carbolin-8-amine | HCID 21362701 | — |
| Reactant | HCID 50999109 | HCID 50999109 | — |
| Product | (S)-5-(6-Chloro-9H-beta-carbolin-8-ylcarbamoyl)-2,2-dimethyl-morpholine-4-carboxylic acid tert-butyl ester | HCID 67164495 | 87% |
Reaction Steps
The desired compound was prepared according to Method C from 6-chloro-9H-β-carboline-8-ylamine and 6,6-dimethyl-morpholine-3,4-dicarboxylic acid 4-tert-butyl ester in 87% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07727985B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-a27e6a4f7bd746fdaef7e84f334dece2 |
| Source note | uspto-grants-2010_06 |