HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl 2-(S)-[N-carbobenzyloxy]amino-3-aminopropionate, hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Z-Dap-OH | HCID 2756313 | — |
| Product | Methyl 2-(S)-[N-carbobenzyloxy]amino-3-aminopropionate, hydrochloride | HCID 13756825 | — |
Reaction Steps
To the compound obtained in Step 1 were added methanol (100 ml) and thionyl chloride (2.4 ml), and the mixture was stirred overnight at room temperature. The solvent was evaporated to give the title compound as a crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07728005B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-8a8273912e574903ba20d785b22b3f70 |
| Source note | uspto-grants-2010_06 |