Dimethyl Sulfate → HCID 21936532, compound

HRID 1241687Notes

Reaction equation

HRID 1241687 reaction equation
[CH3:1][C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[C:7]([CH3:12])[CH:8]=2)[N:3]=1.[CH3:13][O:14][S:15]([O:18]C)(=[O:17])=[O:16]>>[CH3:13][O:14][S:15]([O-:18])(=[O:17])=[O:16].[CH3:13][N+:3]1[C:4]2[C:9](=[CH:8][C:7]([CH3:12])=[CH:6][CH:5]=2)[CH:10]=[CH:11][C:2]=1[CH3:1]

Participants

3

Reactant 2

HCID 6497Dimethyl SulfateHCID 134142,6-Dimethylquinoline

Product 1

HCID 21936532HCID 21936532, compoundYield 190%

Procedure

2,6-Dimethylquinoline (4.78 g, 30 mmol) was alkylated with dimethylsulphate (3.78 g, 30 mmol) as above to give the title compound (7.9 g, 28.5 mmol, 95%).

Sources & evidence

ORD record
ord-ec2c2bc367dc4619872a7de70bb03b9e
Source dataset
uspto-grants-2006_10
Patent number
US07115619B2

Reaction notes

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