HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 10891563, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 5496199 | HCID 5496199 | — |
| Reactant | HCID 21936501 | HCID 21936501 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 10891563 | HCID 10891563 | 65% |
Reaction Steps
A method analogous to Method E-6, applied to 6-chloro-1,3-dihydroxy-10-methyl-10H-acridin-9-one, 18 (52 g, 0.2 mol), dry acetone (1.75 L), potassium carbonate (80 g, 0.58 mol) and iodomethane (175 ml, 0.74 mol) added for 3 hrs reflux gave complete reaction, work-up and recrystallisation gave the title compound (37 g, 0.13 moles, 65%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07115619B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-0435921f77624f1baac3d4f052b803ac |
| Source note | uspto-grants-2006_10 |