HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 178479873, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 11130764 | HCID 11130764 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178479873 | HCID 178479873 | 99.7% |
Reaction Steps
The general procedure (Method K, described below) applied to 6-methoxy-8-methyl-8H-quino[4,3,2-kl]acridine, 31 (400 mg, 1.28 mmol), dry benzene (100 ml) aluminium chloride (900 mg), methanol (100 ml), sat. aq. sodium hydrogen carbonate (40 ml), and ethyl acetate (100 ml) gave the title compound (381 mg, 1.27 mmol, 99.7%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07115619B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-6adbecf0e8db4751a0fa80b699677c7c |
| Source note | uspto-grants-2006_10 |