HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Disulfide → HCID 178507537, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | m-Aminobenzohydrazide | HCID 84178 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178507537 | HCID 178507537 | — |
Reaction Steps
3-Aminobenzhydrazide (5.76 g) was dissolved in ethanol (40 mL), and triethylamine (4.8 mL) and carbon disulfide (2.1 mL) were added to the solution. The mixture was heated under reflux for 4 hrs. The solvent was evaporated, and water was added. The precipitated solids were collected by filtration to give the title compound (5.06 g) as a pale-yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07115635B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-2272d54bcda141169e47c2ffb68a7bea |
| Source note | uspto-grants-2006_10 |