HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → N-Ethyl-3-nitropyridin-4-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | 4-Chloro-3-nitropyridine | HCID 2735781 | — |
| Product | N-Ethyl-3-nitropyridin-4-amine | HCID 21937597 | — |
Reaction Steps
In a manner similar to example 31, the title compound was prepared from 4-chloro-3-nitropyridine, prepared according to published procedure [J. Med. Chem. 1996, 39, 487–493], and ethylamine. 1H-NMR (CDCl3): δ 9.22 (1H, s), 8.30 (1H, d), 8.10 (1H, br s), 6.71 (1H, d), 3.40 (2H, m), 1.39 (3H, t).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07115640B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-9f0af2f569834325bb25c4cc9e1790a3 |
| Source note | uspto-grants-2006_10 |