3'-Aminoacetophenone → HCID 73855130, compound

Participants

Reaction Steps

The title compound was synthesized in a manner similar to that described in Example 146 by condensing 3′-aminoacetophenone with 3-benzyl-5-[5-(2-methoxyethoxy)-3-methylbenzothiazol-2-ylidene]-2-methylthio-4-oxo-2-thiazolium p-toluenesulfonate. 1H-NMR (CDCl3): δ 7.75 (1H, d), 7.60–7.64 (3H, m), 7.28–7.50 (6H, m), 7.24 (1H, d), 6.85 (1H, m), 5.21 (2H, s), 4.18 (2H, m), 3.80 (2H, m), 3.70 (3H, s), 3.48 (3H, s), 2.65 (3H, s); MS(ESI): 546(MH+).

Provenance & Evidence