Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 53269523 | HCID 53269523 | — |
| Product | HCID 13625903 | HCID 13625903 | — |
Reaction Steps
1 g of 5-chloro-2-nitrophenyl-o-tolylamine was added to a solution of 1 g of sodium in 20 ml of methanol, and it was refluxed for 72 hours. Then, it is cooled to 0° C., and the crystalline product is suctioned off.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07115645B2 |
|---|
| Source dataset | uspto-grants-2006_10 |
|---|
| ORD ID | ord-fe5923dfb92742ca8b0a11028d124c5f |
|---|
| Source note | uspto-grants-2006_10 |
|---|
