Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 53269524 | HCID 53269524 | — |
| Product | HCID 67366440 | HCID 67366440 | — |
Reaction Steps
39 g of 5-chloro-2-nitrophenyl-m-tolylamine was added to a solution of 9 g of sodium in 670 ml of methanol, and it was refluxed for 72 hours. Then, it is cooled to 0° C., and the crystalline product is suctioned off.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07115645B2 |
|---|
| Source dataset | uspto-grants-2006_10 |
|---|
| ORD ID | ord-fb5ffb6c760142c8b177d1b4397e25a3 |
|---|
| Source note | uspto-grants-2006_10 |
|---|
