Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Naphthylamine | HCID 7057 | — |
| Reactant | 3-Fluoro-4-nitrophenol | HCID 520948 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 21938092 | HCID 21938092 | — |
Reaction Steps
3 g of 3-fluoro-4-nitrophenol and 8.2 g of 2-naphthylamine were mixed and stirred for 8 hours at 180° C. The raw mixture was taken up in chloroform and washed with 2N aqueous hydrochloric acid. The organic phase was dried on sodium sulfate and concentrated by evaporation in a vacuum. The residue was chromatographed on silica gel.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07115645B2 |
|---|
| Source dataset | uspto-grants-2006_10 |
|---|
| ORD ID | ord-4c4dbd53694545ef9a0a583ba260400c |
|---|
| Source note | uspto-grants-2006_10 |
|---|
