HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 67365433, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 3-Fluoro-4-nitroanisole | HCID 565654 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 67365433 | HCID 67365433 | — |
Reaction Steps
A solution of 2 g of 3-fluoro-4-nitroanisole in 16 ml of aniline was stirred for 24 hours at 140° C. After cooling, it was taken up in ethyl acetate and extracted with 2N aqueous hydrochloric acid. The organic phase was dried on sodium sulfate and concentrated by evaporation in a vacuum. The residue was chromatographed on silica gel.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07115645B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-528adb3758584b11bf22e3a3967124d7 |
| Source note | uspto-grants-2006_10 |