HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 12282158, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 4-Chlorobenzonitrile | HCID 12163 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12282158 | HCID 12282158 | — |
Reaction Steps
10 g of 4-chlorobenzonitrile was suspended in 12 ml of ethanol and dissolved by adding diethyl ether. While being cooled in an ice bath, it was saturated with HCl gas. After 72 hours, precipitated product was suctioned out. The product was washed with diethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07115645B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-e645725a5d734b9fb8466411bedaa264 |
| Source note | uspto-grants-2006_10 |