HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Acetylpiperidine-4-carboxylic acid → HCID 58714535, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Acetylpiperidine-4-carboxylic acid | HCID 117255 | — |
| Reactant | (2S,4EZ)-1-([1,1'-biphenyl]-4-ylcarbonyl)-N'-hydroxy-4-(methoxyimino)-2-pyrrolidinecarboximidamide | HCID 90995821 | — |
| Product | HCID 58714535 | HCID 58714535 | — |
Reaction Steps
Following the general method as outlined in Example 15, starting from (2S,4EZ)-1-([1,1′-biphenyl]-4-ylcarbonyl)-N′-hydroxy-4-(methoxyimino)-2-pyrrolidinecarboximidamide (Intermediate 8) and 1-acetyl-4-piperidinecarboxylic acid, the title compound was obtained in 87% purity by HPLC. MS(ESI+): m/z=488.4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07115639B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-097f507eb3e54c43b8b43085edd72314 |
| Source note | uspto-grants-2006_10 |