HuagongsheHuagongshe Chemistry Print Report · For research reference only
(+-)-3-Phenyllactic acid → HCID 58714523, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (+-)-3-Phenyllactic acid | HCID 3848 | — |
| Reactant | (2S,4EZ)-1-([1,1'-biphenyl]-4-ylcarbonyl)-N'-hydroxy-4-(methoxyimino)-2-pyrrolidinecarboximidamide | HCID 90995821 | — |
| Product | HCID 58714523 | HCID 58714523 | — |
Reaction Steps
Following the general method as outlined in Example 15, starting from (2S,4EZ)-1-([1,1′-biphenyl]-4-ylcarbonyl)-N′-hydroxy-4-(methoxyimino)-2-pyrrolidinecarboximidamide (Intermediate 8) and (2RS)-2-hydroxy-3-phenylpropanoic acid, the title compound was obtained in 78% purity by HPLC. MS(ESI+): m/z=483.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07115639B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-3abb7d89cdff4da18240c64d2d006854 |
| Source note | uspto-grants-2006_10 |