HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → Methyl 2-(2-iodophenyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 2-Iodophenylacetic acid | HCID 2780090 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 2-(2-iodophenyl)acetate | HCID 640185 | 100% |
Reaction Steps
2-Iodophenylacetic acid (1.45 g) was added to a mixture of methanol (100 mL) and acetyl chloride (5 mL). After stirring at room temperature for 3 hours, the solvent was removed and the residue was dried under vacuum giving the desired 2-iodophenylacetic acid methyl ester. Yield=100%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07115741B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-9648dbe8a0734f798b9e731b9c3a0a62 |
| Source note | uspto-grants-2006_10 |