Phthalimide → HCID 90719168, compound

Participants

Reaction Steps

A solution of alcohol (2) (EZ mixture, 51 mg, 0.16 mmol), phtalimide (70 mg, 0.48 mmol), triphenylphosphine polymer bound (158 mg, 0.48 mmol) and diethyl azodicarboxylate (40% in toluene, 205 μl, 0.48 mmol) in tetrahydrofuran (5 ml) was stirred for 2 days. The resin was filtered off and the reaction mixture was concentrated in vacuo. The crude was purified on silica gel preparative chromatography using DCM as eluant.

Provenance & Evidence