HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexylamine → HCID 9899074, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexylamine | HCID 8102 | — |
| Reactant | 3-Bromoaniline | HCID 11562 | — |
| Product | HCID 9899074 | HCID 9899074 | 80.1% |
Reaction Steps
Using the general procedure, 3-bromoaniline (172 mg, 1.0 mmol) was coupled with n-hexylamine (198 μL, 1.5 mmol). Purification of the crude product by column chromatography on silica gel using hexane/ethyl acetate (2:1) as eluent afforded the desired product as a colorless oil (154 mg, 80% yield). Rf=0.4 (hexane/ethyl acetate=2:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07115784B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-0c2b60c606cc4b8cb6b8ea8a59d95a56 |
| Source note | uspto-grants-2006_10 |