Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1243099Generated: October 30, 2026

Hexylamine → HCID 9899074, compound

https://huagongshe.com/reaction/1243099

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHexylamineHCID 8102—
Reactant3-BromoanilineHCID 11562—
ProductHCID 9899074HCID 989907480.1%

Reaction Steps

Using the general procedure, 3-bromoaniline (172 mg, 1.0 mmol) was coupled with n-hexylamine (198 μL, 1.5 mmol). Purification of the crude product by column chromatography on silica gel using hexane/ethyl acetate (2:1) as eluent afforded the desired product as a colorless oil (154 mg, 80% yield). Rf=0.4 (hexane/ethyl acetate=2:1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07115784B2
Source datasetuspto-grants-2006_10
ORD IDord-0c2b60c606cc4b8cb6b8ea8a59d95a56
Source noteuspto-grants-2006_10