HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromotoluene → HCID 9834366, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromotoluene | HCID 7805 | — |
| Reactant | 2-(1-Cyclohexenyl)ethylamine | HCID 76938 | — |
| Product | HCID 9834366 | HCID 9834366 | 95.2% |
Reaction Steps
Using the general procedure, 4-bromotoluene (172 mg, 1.0 mmol) was coupled with 2-(1-cyclohexenyl)ethylamine (209 μL, 1.5 mmol). Purification of the crude product by column chromatography on silica gel using hexane/ethyl acetate (20:1) as eluent afforded the desired product as a colorless oil (205 mg, 95% yield). Rf=0.6 (hexane/ethyl acetate=10:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07115784B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-fb5b7b30ece8478ebda236b401e68c6a |
| Source note | uspto-grants-2006_10 |