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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1243352Generated: October 30, 2026

HCID 86597791, compound → HCID 86597792, compound

https://huagongshe.com/reaction/1243352

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86597791HCID 86597791—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 86597792HCID 8659779296.3%

Reaction Steps

Ethyl [[7-allyl-3-[2-[2-(2,4-dichlorophenyl)-5-isopropyl-4-oxazolyl]ethyl]-1,2-benzisoxazol-6-yl]oxy]acetate (65 mg, 0.12 mmol) was dissolved in ethanol (7.0 mL). To the solution, 10% Pd—C (6 mg) was added. The mixture was stirred for 3 hours under hydrogen atmosphere (and ordinary pressure). After insoluble was filtered off, the filtrate was condensed to give the desired compound (63 mg) as colorless oil in the residue (yield 97%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07119104B2
Source datasetuspto-grants-2006_10
ORD IDord-1d3f83136ec14970a3afd6225e13f7f5
Source noteuspto-grants-2006_10