HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86597791, compound → HCID 86597792, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86597791 | HCID 86597791 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86597792 | HCID 86597792 | 96.3% |
Reaction Steps
Ethyl [[7-allyl-3-[2-[2-(2,4-dichlorophenyl)-5-isopropyl-4-oxazolyl]ethyl]-1,2-benzisoxazol-6-yl]oxy]acetate (65 mg, 0.12 mmol) was dissolved in ethanol (7.0 mL). To the solution, 10% Pd—C (6 mg) was added. The mixture was stirred for 3 hours under hydrogen atmosphere (and ordinary pressure). After insoluble was filtered off, the filtrate was condensed to give the desired compound (63 mg) as colorless oil in the residue (yield 97%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07119104B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-1d3f83136ec14970a3afd6225e13f7f5 |
| Source note | uspto-grants-2006_10 |