HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21925692, compound → HCID 21925676, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21925692 | HCID 21925692 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 21925676 | HCID 21925676 | 73.4% |
Reaction Steps
Dimethyl 2-[2-nitro-4-(3-trifluoroacetamidophenyl)phenyl]malonate (4.4 g) was refluxed overnight in 50 mL 6N hydrochloric acid. The reaction mixture was cooled to room temperature and the solids were collected by vacuum filtration, washed with water, and dried under vacuum to give 2.7 g (73% yield) of 2-[2-nitro-4-(3-trifluoroacetamidophenyl)phenyl]acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07119090B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-3acbab31e06e4608b7fb622a71ef96c1 |
| Source note | uspto-grants-2006_10 |