HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69590511, compound → HCID 15147569, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69590511 | HCID 69590511 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15147569 | HCID 15147569 | 97% |
Reaction Steps
A solution of methyl 4-(4-benzylpiperazin-1-yl)but-2-enoate (10.2 g, 0.04 moles) in methanol was added to 20% palladium hydroxide on carbon and placed under 40 psi hydrogen gas for 7 h. The resulting solution was filtered through celite and evaporated to afford methyl 4-(4-benzylpiperazin-1-yl)butanoate (6.70 g, 97%). MS (ESI+) for m/z 187 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07119098B2 |
| Source dataset | uspto-grants-2006_10 |
| ORD ID | ord-db36e6a078414aba97a341e7960411d2 |
| Source note | uspto-grants-2006_10 |