Dimethylamine → HCID 11777534, compound

HRID 1243633Notes

Reaction equation

HRID 1243633 reaction equation
Cl[C:2]1[CH:3]=[CH:4][C:5]2[NH:6][N:7]=[C:8]3[C:17]4[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=4)[C:11](=[O:18])[C:10]=1[C:9]=23.[CH3:19][NH:20][CH3:21]>N1C=CC=CC=1>[CH3:19][N:20]([CH3:21])[C:2]1[CH:3]=[CH:4][C:5]2[NH:6][N:7]=[C:8]3[C:17]4[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=4)[C:11](=[O:18])[C:10]=1[C:9]=23

Participants

4

Reactant 2

HCID 674DimethylamineHCID 11402576HCID 11402576, compound

Product 1

HCID 11777534HCID 11777534, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Conditions

Temperature
100 °C

Procedure

A mixture of 5-chloroanthra[1,9cd]pyrazol-6(2H)-one (Example 1-B) and dimethylamine in pyridine is heated at 100° C. for 16 hours. The mixture is cooled and evaporated. The residue is chromatographed on silica gel to give the desired compound as yellow solids.

Workup

  1. temperatureThe mixture is cooled
  2. customevaporated
  3. customThe residue is chromatographed on silica gel

Sources & evidence

ORD record
ord-2f44803dd408424c828ac457a01ce5f4
Source dataset
uspto-grants-2006_10
Patent number
US07119114B1

Reaction notes

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